3ZIO
minor-site specific NLS (A28)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 300 |
Collection date | 2010-09-02 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.940, 90.180, 100.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.740 - 2.100 |
R-factor | 0.1835 |
Rwork | 0.182 |
R-free | 0.20200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ial |
RMSD bond length | 0.010 |
RMSD bond angle | 0.980 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.800 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.150 | 0.920 |
Number of reflections | 42561 | |
<I/σ(I)> | 10.5 | 2.2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 7.2 | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.65 M SODIUM CITRATE, 0.1 M HEPES BUFFER (PH 6.5) AND 10 MM DTT |