3ZDI
Glycogen Synthase Kinase 3 Beta complexed with Axin Peptide and Inhibitor 7d
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.147, 76.157, 86.545 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.046 - 2.645 |
R-factor | 0.2036 |
Rwork | 0.201 |
R-free | 0.24230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o9u |
RMSD bond length | 0.003 |
RMSD bond angle | 0.750 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.050 | 2.800 |
High resolution limit [Å] | 2.640 | 2.640 |
Rmerge | 0.070 | 0.860 |
Number of reflections | 14488 | |
<I/σ(I)> | 18 | 2.3 |
Completeness [%] | 98.8 | 97 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M 2-(N-MORPHOLINO)ETHANESULFONIC ACID (MES), PH 6.5, 12% (W/V) PEG 20000 |