3ZD6
Snapshot 1 of RIG-I scanning on RNA duplex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 287 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.474, 78.017, 225.104 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.800 |
R-factor | 0.22444 |
Rwork | 0.222 |
R-free | 0.27896 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ykg |
RMSD bond length | 0.013 |
RMSD bond angle | 1.562 |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.060 | 0.710 |
Number of reflections | 21820 | |
<I/σ(I)> | 16.2 | 1.8 |
Completeness [%] | 99.5 | 99.3 |
Redundancy | 5 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | pH 9 |