3ZC0
Structure of AfC3PO - duplex RNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-07-03 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 183.060, 183.060, 198.120 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 83.091 - 2.982 |
R-factor | 0.2103 |
Rwork | 0.208 |
R-free | 0.25720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zc1 |
RMSD bond length | 0.021 |
RMSD bond angle | 1.242 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 123.780 | 3.060 |
High resolution limit [Å] | 2.980 | 2.980 |
Rmerge | 0.110 | 0.830 |
Number of reflections | 78522 | |
<I/σ(I)> | 14.6 | 3.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.1 | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 2.7 M 1,6-HEXANEDIOL, 200 MM AMMONIUM CHLORIDE, 10 MM MGCL2, 50 MM HEPES PH 8.0, 5 MM DTT. |