3ZBD
Structure of TGEV nsp1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 110 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 1 |
Unit cell lengths | 35.640, 36.090, 42.270 |
Unit cell angles | 91.49, 108.85, 94.20 |
Refinement procedure
Resolution | 26.050 - 1.490 |
R-factor | 0.1763 |
Rwork | 0.175 |
R-free | 0.20890 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.060 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.400 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.060 | 0.480 |
Number of reflections | 30811 | |
<I/σ(I)> | 14.3 | 3 |
Completeness [%] | 96.6 | 95.4 |
Redundancy | 4 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5%(V/VOL) PEG 4000, 200MM AMMONIUM CHLORIDE, 30MM HEPES, 30MM MES, PH 6.2 | |||
1 | 5%(V/VOL) PEG 4000, 200MM AMMONIUM CHLORIDE, 30MM HEPES, 30MM MES, PH 6.2 |