3X3S
Recombinant thaumatin in the presence of 1.5M PST at 293K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2014-10-12 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.00 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 58.506, 58.506, 151.713 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.724 - 1.460 |
R-factor | 0.1093 |
Rwork | 0.108 |
R-free | 0.13320 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.064 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.490 |
High resolution limit [Å] | 1.460 | 1.460 |
Rmerge | 0.046 | 0.491 |
Number of reflections | 46801 | |
<I/σ(I)> | 73.99 | 7.26 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.5 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 0.05M ADA, 1.5 M K-Na TARTRATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |