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3X3P

Recombinant thaumatin in the presence of 0.75M PST at 293K

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL26B1
Synchrotron siteSPring-8
BeamlineBL26B1
Temperature [K]293
Detector technologyCCD
Collection date2014-10-12
DetectorRIGAKU SATURN A200
Wavelength(s)1.00
Spacegroup nameP 41 21 2
Unit cell lengths58.519, 58.519, 151.589
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution28.729 - 1.480
R-factor0.1084
Rwork0.107
R-free0.13450
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle1.070
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Refinement softwarePHENIX ((phenix.refine: 1.9_1692))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.510
High resolution limit [Å]1.4801.480
Rmerge0.0490.409
Number of reflections44959
<I/σ(I)>75.028.41
Completeness [%]99.9100
Redundancy13.212.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72930.05M ADA, 0.75M K-Na TARTRATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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