3WZS
Crystal structure of Trx3 domain of UGGT (detergent-bound form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2014-06-14 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97921 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 46.200, 93.600, 81.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.700 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.24700 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.465 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXS |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.082 | 0.366 |
Number of reflections | 19829 | |
<I/σ(I)> | 47.9 | 7.2 |
Completeness [%] | 98.5 | 98.9 |
Redundancy | 6.8 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 289 | 23% PEG3350, 0.1M Tris-HCl (pH 7.0), 0.2M ammonium acetate, VAPOR DIFFUSION, HANGING DROP, temperature 289K |