3WVZ
Crystal structure of Hikeshi, a new nuclear transport receptor of Hsp70
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 90 |
Detector technology | AREA DETECTOR |
Collection date | 2013-11-08 |
Wavelength(s) | 0.9192 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 61.138, 137.839, 97.902 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.909 - 1.880 |
R-factor | 0.2082 |
Rwork | 0.207 |
R-free | 0.22780 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.865 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 |
High resolution limit [Å] | 1.880 | 1.880 |
Number of reflections | 19445 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293.15 | 0.1M Tris-HCl (pH 7.4), 1M ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |