3WVU
Crystal Structure of RuCO/apo-R52CFr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-02-17 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.5418 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.575, 181.575, 181.575 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.260 - 1.920 |
R-factor | 0.15985 |
Rwork | 0.158 |
R-free | 0.19272 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.023 |
RMSD bond angle | 2.081 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.920 | 1.920 |
Number of reflections | 19140 | |
<I/σ(I)> | 48.6 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 20.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 1M ammonium sulfate, 20mM cadmium sulfate, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |