3WTC
Crystal structure of Gox2036
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-02-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.075 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 117.840, 58.098, 67.246 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.220 - 1.650 |
| R-factor | 0.14907 |
| Rwork | 0.148 |
| R-free | 0.17376 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3v2g |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.071 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.690 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Number of reflections | 53193 | |
| Completeness [%] | 99.8 | 99.46 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 293 | PEG3350, HEPES, Proline, pH 7.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
