3WP8
Acinetobacter sp. Tol 5 AtaA C-terminal Ylhead fused to GCN4 adaptors (Chead)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 63 |
Unit cell lengths | 54.406, 54.406, 210.732 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.240 - 1.970 |
R-factor | 0.1782 |
Rwork | 0.175 |
R-free | 0.22980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ntn |
RMSD bond length | 0.018 |
RMSD bond angle | 1.764 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 1.970 | 4.310 | 2.000 |
Rmerge | 0.069 | 0.038 | 0.421 |
Number of reflections | 24269 | ||
<I/σ(I)> | 14.8 | ||
Completeness [%] | 99.2 | 98 | 99 |
Redundancy | 11.2 | 11.1 | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 3.6 | 298 | 3% PEG 6000, 1.0M NaCl, 0.1M Na-acetate, pH 3.6, vapor diffusion, hanging drop, temperature 298K |