3WMR
Crystal structure of VinJ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 |
Unit cell lengths | 52.870, 72.620, 75.450 |
Unit cell angles | 114.02, 98.39, 98.50 |
Refinement procedure
Resolution | 50.960 - 1.950 |
R-factor | 0.16737 |
Rwork | 0.165 |
R-free | 0.20576 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3nwo |
RMSD bond length | 0.008 |
RMSD bond angle | 1.214 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.960 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 63636 | |
Completeness [%] | 88.7 | 65.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 278 | 0.2M lithium acetate, 20% polyethylene glycol 3350, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 278K |