3WMP
Crystal structure of SLL-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-06-15 |
Detector | ADSC QUANTUM 270 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.030, 189.950, 57.050 |
Unit cell angles | 90.00, 110.55, 90.00 |
Refinement procedure
Resolution | 94.980 - 2.000 |
R-factor | 0.251 |
Rwork | 0.251 |
R-free | 0.27100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ccv |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 69338 | |
Completeness [%] | 99.4 | 98.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 293 | MPD, calcium formate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |