3WMI
Crystal structure of EIAV wild type gp45
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2011-05-09 |
| Detector | ENRAF-NONIUS |
| Wavelength(s) | 0.9794 |
| Spacegroup name | P 63 |
| Unit cell lengths | 47.051, 47.051, 101.918 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 31.824 - 1.900 |
| R-factor | 0.1778 |
| Rwork | 0.175 |
| R-free | 0.22920 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.788 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 31.824 | 1.930 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 10074 | |
| Completeness [%] | 11.0 | 95 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 5.5 | 293 | 0.1M Bis-Tris, 2M NaCl, pH 5.5, EVAPORATION, temperature 293K |
