3WIL
Crystal structure of the CK2alpha/compound3 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2011-10-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.092, 78.991, 82.518 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.030 - 2.900 |
R-factor | 0.21169 |
Rwork | 0.204 |
R-free | 0.28077 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3war |
RMSD bond length | 0.019 |
RMSD bond angle | 1.824 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 57.060 |
High resolution limit [Å] | 2.900 |
Number of reflections | 7410 |
Completeness [%] | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 25% ethyleneglycol, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K |