3WIK

Crystal structure of the CK2alpha/compound10 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	95
Detector technology	CCD
Collection date	2011-11-11
Detector	RAYONIX MX225HE
Wavelength(s)	0.90
Spacegroup name	P 21 21 21
Unit cell lengths	48.382, 79.451, 82.888
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.785 - 1.995
R-factor	0.1656
Rwork	0.163
R-free	0.21140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.017
RMSD bond angle	1.852
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AMoRE
Refinement software	REFMAC (5.5.0102)

Data quality characteristics

	Overall
Low resolution limit [Å]	57.030
High resolution limit [Å]	1.850
Number of reflections	27524
Completeness [%]	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	8	277	25% ethyleneglycol, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 277K