3WAO
Crystal structure of Atg13 LIR-fused human LC3B_2-119
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 2012-01-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98000 |
Spacegroup name | P 41 |
Unit cell lengths | 64.569, 64.569, 130.332 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.440 - 2.600 |
R-factor | 0.22608 |
Rwork | 0.223 |
R-free | 0.29404 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vtu |
RMSD bond length | 0.011 |
RMSD bond angle | 1.801 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.440 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.068 | 0.740 |
Number of reflections | 16435 | |
<I/σ(I)> | 14.4 | 2.4 |
Completeness [%] | 99.9 | 99.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Sodium citrate tribasic dihydrate 10% PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 293K |