3W9U
Crystal structure of Lipk107
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.075 |
Spacegroup name | P 32 |
Unit cell lengths | 65.484, 65.484, 63.871 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
R-factor | 0.18124 |
Rwork | 0.179 |
R-free | 0.21473 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ex9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.049 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.700 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 19653 | |
Completeness [%] | 95.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | Sodium citrate, PEG4000,2-propanol, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |