3W9P
Crystal structure of monomeric FraC (second crystal form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-23 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.980, 60.510, 80.840 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.270 - 2.100 |
R-factor | 0.1646 |
Rwork | 0.162 |
R-free | 0.21560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3lim |
RMSD bond length | 0.011 |
RMSD bond angle | 1.441 |
Data reduction software | MOSFLM |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.1) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.270 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.104 | 0.366 |
Number of reflections | 17493 | |
<I/σ(I)> | 13.5 | 4.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.4 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | 100mM sodium citrate, 20% isopropanol, 16% PEG 4000, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |