3W6S
yeast N-acetyltransferase Mpr1 involved in oxidative stress tolerance via proline metabolism
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-06-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9793 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 83.862, 83.862, 193.819 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.271 - 1.900 |
R-factor | 0.1706 |
Rwork | 0.166 |
R-free | 0.18720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3w91 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.015 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.300 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.060 | 0.287 |
Number of reflections | 61875 | |
<I/σ(I)> | 2.4 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.9 | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |