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3W5X

MamM-CTD

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-4
Synchrotron siteESRF
BeamlineID14-4
Temperature [K]100
Collection date2011-11-29
DetectorADSC QUANTUM 315r
Wavelength(s)0.939
Spacegroup nameC 2 2 21
Unit cell lengths36.882, 94.559, 53.542
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution47.280 - 1.600
R-factor0.1714
Rwork0.170
R-free0.20650
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3byp
RMSD bond length0.025
RMSD bond angle2.149
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.630
High resolution limit [Å]1.6004.3401.600
Rmerge0.0580.0390.480
Number of reflections12559
<I/σ(I)>18.4
Completeness [%]98.285.883.4
Redundancy6.15.14.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.529325% PEG 4000, 0.2M Ammonium sulfate, 0.1M Sodium acetate , pH 5.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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