3W08
Crystal structure of aldoxime dehydratase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Detector technology | CCD |
Collection date | 2004-02-29 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 152.946, 84.458, 76.360 |
Unit cell angles | 90.00, 114.32, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.158 |
Rwork | 0.157 |
R-free | 0.18900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a16 |
RMSD bond length | 0.021 |
RMSD bond angle | 2.462 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.800 |
Number of reflections | 81721 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |