Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Collection date | 2005-07-12 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97923 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.487, 107.581, 117.711 |
| Unit cell angles | 90.00, 102.44, 90.00 |
Refinement procedure
| Resolution | 45.390 - 2.490 |
| R-factor | 0.19453 |
| Rwork | 0.191 |
| R-free | 0.25452 |
| Structure solution method | MAD |
| RMSD bond length | 0.028 |
| RMSD bond angle | 2.123 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.390 | 2.590 |
| High resolution limit [Å] | 2.490 | 2.500 |
| Number of reflections | 47040 | |
| <I/σ(I)> | 3.9 | |
| Completeness [%] | 99.8 | 99.9 |
| Redundancy | 4.1 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | PEG 3350, sodium acetate, benzamidine, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | PEG 3350, sodium acetate, benzamidine, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
