3VYU
Crystal structure of the HypC-HypD-HypE complex (form II)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-24 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 114.677, 121.461, 67.354 |
Unit cell angles | 90.00, 97.20, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.850 |
High resolution limit [Å] | 2.750 | 2.750 |
Number of reflections | 21147 | |
<I/σ(I)> | 19.8 | 1.9 |
Completeness [%] | 88.7 | 55.7 |
Redundancy | 3.6 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.7 | 293 | 0.1M Tris-HCl, 12-16%(w/v) PEG8000, 2% ethylene glycol, pH 8.7, VAPOR DIFFUSION, SITTING DROP, temperature 293K |