3VWW
Crystal structure of a0-domain of P5 from H. sapiens
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-01-21 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 0.90 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 90.461, 43.241, 61.245 |
| Unit cell angles | 90.00, 101.29, 90.00 |
Refinement procedure
| Resolution | 30.030 - 1.930 |
| R-factor | 0.1757 |
| Rwork | 0.173 |
| R-free | 0.23170 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.028 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.030 | 2.050 |
| High resolution limit [Å] | 1.930 | 1.930 |
| Number of reflections | 17678 | |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 3.7 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.7 | 293 | 5% PEG 4000, 50mM sodium phosphate (pH 6.7), VAPOR DIFFUSION, temperature 293K |
