3VU9
Crystal Structure of Psy3-Csm2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-25 |
Detector | ADSC Quantum 270r |
Wavelength(s) | 1.00000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 134.560, 50.403, 76.350 |
Unit cell angles | 90.00, 102.92, 90.00 |
Refinement procedure
Resolution | 36.000 - 1.750 |
R-factor | 0.1847 |
Rwork | 0.182 |
R-free | 0.23119 |
Structure solution method | SAD |
RMSD bond length | 0.024 |
RMSD bond angle | 2.280 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.500 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.048 | 0.485 |
Number of reflections | 45389 | |
<I/σ(I)> | 14.1 | 2.2 |
Completeness [%] | 90.0 | |
Redundancy | 3.8 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Hanging Drop Vapor Diffusion | 7 | 293 | 0.1M Tris-HCl, 30% Ethylene glycol(in case of Se-Met derivative, 25%), 5% polyethylene glycol, pH 7.0, Hanging Drop Vapor Diffusion, temperature 293K |