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3VPZ

Crystal structure of glucokinase from Antarctic psychrotroph at 1.69A

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSAGA-LS BEAMLINE BL07
Synchrotron siteSAGA-LS
BeamlineBL07
Temperature [K]100
Detector technologyCCD
Collection date2011-08-31
DetectorRIGAKU SATURN A200
Wavelength(s)1.1
Spacegroup nameP 31 2 1
Unit cell lengths98.610, 98.610, 59.730
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution18.560 - 1.690
R-factor0.20379
Rwork0.201
R-free0.24801
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1q18
RMSD bond length0.004
RMSD bond angle0.783
Data reduction softwareCrystalClear
Data scaling softwareCrystalClear
Phasing softwareMOLREP
Refinement softwareREFMAC (5.6.0117)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]19.390
High resolution limit [Å]1.6901.690
Rmerge0.075
Number of reflections36190
<I/σ(I)>14.3
Completeness [%]95.895.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.52930.2M Trimethylamine N-oxide dihydrate, 20% PEGMME 2000, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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