3VLA
Crystal structure of edgp
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Detector technology | CCD |
Collection date | 2008-06-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.8 |
Spacegroup name | P 62 |
Unit cell lengths | 130.102, 130.102, 44.544 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 0.950 |
R-factor | 0.12847 |
Rwork | 0.128 |
R-free | 0.14559 |
Structure solution method | MIR |
RMSD bond length | 0.016 |
RMSD bond angle | 1.776 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 0.920 |
Number of reflections | 272047 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |