3VL9
Crystal structure of xeg-xyloglucan
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Detector technology | CCD |
| Collection date | 2010-01-23 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 1 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 62.757, 79.283, 80.374 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.200 |
| R-factor | 0.12881 |
| Rwork | 0.127 |
| R-free | 0.16288 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3vl8 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.657 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.200 |
| Number of reflections | 120607 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
