3VL9
Crystal structure of xeg-xyloglucan
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Detector technology | CCD |
Collection date | 2010-01-23 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.757, 79.283, 80.374 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.200 |
R-factor | 0.12881 |
Rwork | 0.127 |
R-free | 0.16288 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vl8 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.657 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.200 |
Number of reflections | 120607 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |