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3VKN

Galectin-8 N-terminal domain in free form

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2011-07-23
DetectorRIGAKU RAXIS VII
Wavelength(s)1.5418
Spacegroup nameP 21 21 21
Unit cell lengths54.610, 62.470, 80.910
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution22.550 - 1.980
Rwork0.204
R-free0.25100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2yv8
RMSD bond length0.005
RMSD bond angle1.300
Data reduction softwareCrystalClear
Data scaling softwareCrystalClear
Phasing softwareMOLREP
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.050
High resolution limit [Å]1.9801.980
Rmerge0.0560.304
Number of reflections19768
<I/σ(I)>14.44.9
Completeness [%]99.5100
Redundancy5.15.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP9.529330%(v/v) PEG 400, 0.1M CHES, pH 9.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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