3VIB
Structural basis for multidrug recognition and antimicrobial resistance by MTRR, an efflux pump regulator from Neisseria Gonorrhoeae
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9797, 0.9798, 1.02 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 218.300, 84.600, 58.100 |
Unit cell angles | 90.00, 103.90, 90.00 |
Refinement procedure
Resolution | 45.460 - 2.400 |
Rwork | 0.212 |
R-free | 0.25600 |
Structure solution method | MAD |
RMSD bond length | 0.008 |
RMSD bond angle | 19.200 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.460 | 2.550 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 39412 | |
Completeness [%] | 97.8 | 98.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 10.5 | 1.7M NA/K PHOSPHATE, 0.18M LITHIUM SULFATE, 0.1M CAPS, PH 10.5, VAPOR DIFFUSION, HANGING DROP, |