3VH8
KIR3DL1 in complex with HLA-B*5701
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9536 |
Spacegroup name | P 1 |
Unit cell lengths | 66.248, 66.374, 93.361 |
Unit cell angles | 100.56, 92.83, 101.56 |
Refinement procedure
Resolution | 35.850 - 1.800 |
R-factor | 0.2126 |
Rwork | 0.211 |
R-free | 0.23730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 2RFX and 1IM9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.221 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.257 | 0.257 |
Number of reflections | 136837 | |
<I/σ(I)> | 20.8 | 3 |
Completeness [%] | 94.6 | 87.8 |
Redundancy | 3.7 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 294 | 16% PEG 3350, 2% tacsimate pH 5.0, 0.1M tri-sodium citrate pH 5.6., VAPOR DIFFUSION, HANGING DROP, temperature 294K |