3VEB
Crystal Structure of Matp-matS
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98037,0.98047,0.91904 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 102.300, 102.300, 193.570 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.080 - 2.800 |
R-factor | 0.266 |
Rwork | 0.266 |
R-free | 0.28300 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.500 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 96.700 |
High resolution limit [Å] | 2.800 |
Number of reflections | 14660 |
Completeness [%] | 95.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 20% PEG3000, 0.2 M calcium chloride, 0.1 M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |