3VD2
structure of p73 DNA binding domain tetramer modulates p73 transactivation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2010-06-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 158.400, 91.127, 137.475 |
Unit cell angles | 90.00, 90.20, 90.00 |
Refinement procedure
Resolution | 45.690 - 4.000 |
R-factor | 0.248 |
Rwork | 0.248 |
R-free | 0.28400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kmd |
RMSD bond length | 0.010 |
RMSD bond angle | 1.900 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 4.140 |
High resolution limit [Å] | 4.000 | 4.000 |
Number of reflections | 16649 | |
<I/σ(I)> | 10.6 | 3.8 |
Completeness [%] | 99.2 | 99.6 |
Redundancy | 5.9 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 0.1M Bis-tris, 0.1M Ammonium acetate, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K, pH 6.5 |