3VD1
structure of p73 DNA binding domain tetramer modulates p73 transactivation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 200 |
Detector technology | CCD |
Collection date | 2010-01-01 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 82.540, 104.200, 123.223 |
Unit cell angles | 90.00, 96.55, 90.00 |
Refinement procedure
Resolution | 19.990 - 2.950 |
R-factor | 0.239 |
Rwork | 0.239 |
R-free | 0.28500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kmd |
RMSD bond length | 0.009 |
RMSD bond angle | 1.700 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.060 |
High resolution limit [Å] | 2.950 | 2.950 |
Number of reflections | 41946 | |
<I/σ(I)> | 20.1 | 3.2 |
Completeness [%] | 96.1 | 96.5 |
Redundancy | 6.2 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.1 | 298 | 0.1M MES, 0.1M Na acetate, pH 6.1, temperature 298.0K |