3V6N
Crystal structure of a plant albumin from Cicer Arietinum showing hemagglutination
Replaces: 3S0LExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 2005-02-03 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 71.246, 73.360, 87.174 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.940 - 2.200 |
R-factor | 0.18155 |
Rwork | 0.179 |
R-free | 0.22580 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3lp9 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.227 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.100 | 0.290 |
Number of reflections | 23739 | |
<I/σ(I)> | 3.17 | |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 3.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 0.1M sodium cacodylate, pH 6.5, 0.2M sodium acetate, 18% w/v polyethylene glycol 8000, VAPOR DIFFUSION, HANGING DROP, temperature 295K |