3V5Z
Structure of FBXL5 hemerythrin domain, C2 cell, grown anaerobically
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-19 |
Detector | ADSC Q315 |
Wavelength(s) | 0.97929 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 60.442, 76.051, 77.433 |
Unit cell angles | 90.00, 112.12, 90.00 |
Refinement procedure
Resolution | 33.830 - 2.185 |
R-factor | 0.1794 |
Rwork | 0.177 |
R-free | 0.22280 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3v5x |
RMSD bond length | 0.008 |
RMSD bond angle | 1.012 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.240 |
High resolution limit [Å] | 2.184 | 5.970 | 2.184 |
Rmerge | 0.062 | 0.039 | 0.552 |
Number of reflections | 16703 | ||
<I/σ(I)> | 14.9 | ||
Completeness [%] | 99.7 | 95 | 100 |
Redundancy | 4 | 3.6 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 12% PEG 6000, 0.1 M HEPES, 30% ethylene glycol, 2M Na(2)S(2)O(4), pH 6.5, vapor diffusion, hanging drop, temperature 293K |