3V4Q
Structure of R335W mutant of human Lamin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2010-11-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97690 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 90.499, 90.499, 75.425 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.590 - 3.060 |
R-factor | 0.2762 |
Rwork | 0.275 |
R-free | 0.28220 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.030 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 75.400 |
High resolution limit [Å] | 3.060 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 277 | 15% Ethanol, 0.1M Citrate pH 5.5, 0.2 M Litium Sulfate, VAPOR DIFFUSION, SITTING DROP, temperature 277K |