3V46
Crystal Structure of Yeast Cdc73 C-Terminal Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-22 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 53.324, 53.324, 130.223 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.706 - 1.549 |
R-factor | 0.1744 |
Rwork | 0.172 |
R-free | 0.21040 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.068 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX (1.6.1_357) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.580 |
High resolution limit [Å] | 1.549 | 4.210 | 1.549 |
Rmerge | 0.054 | 0.043 | 0.380 |
Number of reflections | 28111 | ||
<I/σ(I)> | 17.5 | ||
Completeness [%] | 99.3 | 93.7 | 97.8 |
Redundancy | 7.1 | 6.8 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | PEG 8000, pH 8.0, VAPOR DIFFUSION, temperature 293K |
1 | VAPOR DIFFUSION | 8 | 293 | PEG 8000, pH 8.0, VAPOR DIFFUSION, temperature 293K |