3V32
Crystal structure of MCPIP1 N-terminal conserved domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-20 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1 |
Spacegroup name | P 41 |
Unit cell lengths | 56.350, 56.350, 113.238 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.940 - 2.000 |
R-factor | 0.2059 |
Rwork | 0.202 |
R-free | 0.24440 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.075 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.940 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.079 | 0.274 |
Number of reflections | 21614 | |
<I/σ(I)> | 17.5 | 2 |
Completeness [%] | 90.6 | 51.5 |
Redundancy | 6.2 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 0.1M Bis-Tris, 7% PEG 3350, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |