3V0J
Crystal structure of Ciona intestinalis voltage sensor-containing phosphatase (Ci-VSP), residues 241-576(C363S), Deletion of 401-405
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.1158 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.562, 76.804, 84.007 |
Unit cell angles | 90.00, 92.73, 90.00 |
Refinement procedure
Resolution | 83.910 - 1.720 |
R-factor | 0.18712 |
Rwork | 0.185 |
R-free | 0.22239 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB: 3V0D |
RMSD bond length | 0.008 |
RMSD bond angle | 1.107 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.780 |
High resolution limit [Å] | 1.720 | 1.720 |
Rmerge | 0.116 | 0.740 |
Number of reflections | 68903 | |
<I/σ(I)> | 14.4 | 2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 17.5-22.5% PEG 2000, 0.1 M ammonium dihydrophosphate, 0.1 M Tris-HCl, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |