3UXN
Crystal Structure of Rat DNA Polymerase Beta, Wild Type Apoenzyme
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-04-08 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 77.946, 67.447, 83.357 |
Unit cell angles | 90.00, 116.14, 90.00 |
Refinement procedure
Resolution | 15.002 - 2.500 |
R-factor | 0.2554 |
Rwork | 0.250 |
R-free | 0.31660 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.271 |
Data reduction software | HKL-2000 |
Data scaling software | d*TREK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6.2_432)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 15.002 | 3.069 | 2.567 |
High resolution limit [Å] | 2.500 | 2.937 | 2.500 |
Number of reflections | 22615 | ||
Completeness [%] | 83.9 | 89 | 77 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 296 | PEG 3350, MES, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 296K |