3US3

Recombinant rabbit skeletal calsequestrin-MPD complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.000
Spacegroup name	C 2 2 21
Unit cell lengths	59.214, 144.811, 110.471
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.906 - 1.738
R-factor	0.1984
Rwork	0.197
R-free	0.23190
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	0.931
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX ((phenix.refine: 1.6.1_357))

Data quality characteristics

	Overall
Low resolution limit [Å]	38.906
High resolution limit [Å]	1.738
Number of reflections	48166

Crystallization Conditions

crystal ID	method	pH	temperature	details
1