3UME
Structure of pB intermediate of Photoactive yellow protein (PYP) at pH 7
Experimental procedure
Experimental method | LAUE |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-ID-B |
Synchrotron site | APS |
Beamline | 14-ID-B |
Temperature [K] | 293 |
Detector technology | CCD |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 - 1.2 |
Spacegroup name | P 63 |
Unit cell lengths | 66.900, 66.900, 40.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 1.800 |
R-factor | 0.146 |
Rwork | 0.120 |
R-free | 0.14600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2phy |
RMSD bond length | 0.005 |
RMSD bond angle | 1.485 |
Data reduction software | XFIT |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.600 |
Number of reflections | 10000 |
Completeness [%] | 100.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 3.0 M Ammonium Sulfate, 50 mM Sodium Phosphate, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 293K |