3UK9
Galactose-specific lectin from Dolichos lablab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-06-19 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 73.990, 84.130, 93.159 |
Unit cell angles | 89.92, 76.01, 77.00 |
Refinement procedure
Resolution | 90.170 - 3.110 |
R-factor | 0.2537 |
Rwork | 0.251 |
R-free | 0.30649 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bjq |
RMSD bond length | 0.006 |
RMSD bond angle | 0.960 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.170 | 3.190 |
High resolution limit [Å] | 3.110 | 3.110 |
Rmerge | 0.096 | 0.480 |
Number of reflections | 41323 | |
<I/σ(I)> | 11.3 | 1.9 |
Completeness [%] | 94.3 | 93.7 |
Redundancy | 5.7 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 289 | 30% PEG 6K, 100mM MES, 5% MPD , pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 289K |