3UJG
Crystal structure of SnRK2.6 in complex with HAB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-30 |
Detector | MARRESEARCH |
Wavelength(s) | 1.0 |
Spacegroup name | I 4 |
Unit cell lengths | 154.835, 154.835, 70.966 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.780 - 2.600 |
R-factor | 0.2092 |
Rwork | 0.207 |
R-free | 0.23810 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.264 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (1.3.2) |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 26409 | |
Completeness [%] | 83.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 298 | 1.2 M ammonium sulphate, 2% (w/v) PEG 1000, 3% (w/v) trimethylamine N-oxide dihydrate, pH 8.0, VAPOR DIFFUSION, temperature 298K |