3UE8

Kynurenine Aminotransferase II Inhibitors

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E SUPERBRIGHT
Temperature [K]	93
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	63.616, 116.597, 129.267
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.430 - 3.220
R-factor	0.2038
Rwork	0.200
R-free	0.27480
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.330
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	AMoRE
Refinement software	BUSTER (2.11.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	100.000
High resolution limit [Å]	3.200
Number of reflections	16095
Completeness [%]	99.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1