3UDB
Crystal structure of SnRK2.6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.03887 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 228.094, 98.793, 113.103 |
Unit cell angles | 90.00, 98.48, 90.00 |
Refinement procedure
Resolution | 37.076 - 2.567 |
R-factor | 0.2376 |
Rwork | 0.236 |
R-free | 0.25940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fh9 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.596 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.670 |
High resolution limit [Å] | 2.567 | 2.580 |
Number of reflections | 78271 | |
Completeness [%] | 99.4 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291 | 0.1M Tris, 19% PEG4000, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |