3UD9
Crystal Structure Analysis of FGF1-Disaccharide(NI23) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-01-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 113.574, 46.930, 96.708 |
Unit cell angles | 90.00, 125.71, 90.00 |
Refinement procedure
Resolution | 78.520 - 2.340 |
R-factor | 0.21609 |
Rwork | 0.212 |
R-free | 0.25184 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rg8 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.453 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | EPMR |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.520 | 2.450 |
High resolution limit [Å] | 2.340 | 2.340 |
Rmerge | 0.069 | 0.330 |
Number of reflections | 16907 | |
<I/σ(I)> | 8.6 | 2.18 |
Completeness [%] | 96.0 | 86.83 |
Redundancy | 3.8 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 2M (NH4)HPO4, 0.1M sodium acetate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |